kitchenchemistry

I go over how to make nickel hydrazine nitrate and show some tests How To Make Nickel Hydrazine Nitrate: Req. chemicals: - 20.0g hydrazine sulfate - 14.5g NaOH - 100ml of absolute isopropyl alcohol - some nickel nitrate, i made mine from old coins. first step is to freebase the hydrazine sulfate into alcoholic hydrazine. then, add nickel nitrate to the concentrated freebase at a temperature of about 60c. In the video I did a temp of 30c because I've burnt the NHN before, turning it black, and it was kinda scary watching an explosive boil. adding dextrin will increase the bulk density from 0.9g/cm3 to 1.2g/cm3, however, if you add more than 1% it will turn blue and sticky like I showed in the video. Also, if you use too much alcohol and your hydrazine freebase is too dilute, the complex will not form and you'll get some blue compound. at the end of the video I show the detonation of nhn vs the deflagration of nhn

HYDRAZINE IS CARCINOGENIC. DO NOT REATTEMPT UNLESS YOU'RE A PROFESSIONAL I go over how to make hydrazine sulfate using bleach and other easily accessible materials. I follow the procedure in Leonid Lerners book "A smallscale synthesis to laboratory reagents" at a 72% scale. Needed reagents: 550 mls or 582g of 8% bleach 55g NaOH (draincleaner) 40g Urea (found in icepacks / fertilizer) ~0.8g gelatin 140mls 32% HCl (muriatic acid) 91-96% Sulpheric Acid (draincleaner) Check out my other video on the synthesis of Nickel Hydrazine Nitrate to put this to use.