Make Concentrated Ammonia
In this video we make ammonia gas and dissolve it water from various chemicals easily accessible to the amateur.
The first method is merely boiling household ammonia solution that's domestically available from the local supermarket. The ammonia boiled out is lead into cold water where it can be dissolved. While this did work the yield was quite low at around 2.5g per 100mL of household ammonia solution. From the 600mL of ammonia solution used only about 15g was obtained.
The second method was to revisit the classic method to produce sodium nitrate from ammonium nitrate and sodium hydroxide by dissolving them both separately in water and then mixing them together and trying to boil out the ammonia. This worked terribly and i got almost no yield at all.
The third method that seemed to work the best was to react urea and sodium hydroxide in water. This reaction was well-behaved, steady and easily performed with domestically available chemicals. Starting from 200mL water, 90g urea and 120g sodium hydroxide, about 38.6g of ammonia was obtained.
I intend to use the ammonia in a future project to make nitric acid.
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Make a Silver Oxide Zinc Battery
In this video we make a silver oxide or silver zinc battery.
Related videos:
Restoring Silver by electrochemistry: https://www.youtube.com/watch?v=57iwtmT4LNQ
Toning Silver by Anodization : https://www.youtube.com/watch?v=GajkqaSr01c
Make zinc powder: https://www.youtube.com/watch?v=3X9c6epL7HQ
Make silver powder: https://youtu.be/WRgSviGuEFY
Donate to NurdRage!
Through Patreon (preferred): https://www.patreon.com/NurdRage
Glassware generously provided by http://www.alchemylabsupply.com/
Use the discount code "nurdrage" for a 5% discount.
Twitter: https://twitter.com/NurdRage
Reddit: https://www.reddit.com/r/NurdRage/
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Make Silver Powder by Electrochemistry
In this video we make silver powder using electrochemistry.
The process is pretty simple. Make a solution of 1g silver nitrate in 50mL water. Submerge an anode made of pure silver (i'm using silver coins) and a cathode of carbon. Connect the anode (silver) to the positive terminal of a variable power supply and connect the cathode (carbon) to the negative terminal. Apply a current and raise it until the cathode just starts to bubble hydrogen and then lower it about 25%. Magnetic stirring and a stir bar should be applied to constantly shred the silver dendrites as they grow.
Eventually the anode will be consumed and the solution is decanted to recover the silver powder. The silver powder is washed a few times with water and then dried by heating on the hot plate.
Related videos:
Restoring Silver by electrochemistry: https://www.youtube.com/watch?v=57iwtmT4LNQ
Toning Silver by Anodization : https://www.youtube.com/watch?v=GajkqaSr01c
Make zinc powder: https://www.youtube.com/watch?v=3X9c6epL7HQ
Donate to NurdRage!
Through Patreon (preferred): https://www.patreon.com/NurdRage
Glassware generously provided by http://www.alchemylabsupply.com/
Use the discount code "nurdrage" for a 5% discount.
Twitter: https://twitter.com/NurdRage
Reddit: https://www.reddit.com/r/NurdRage/
Instagram: https://www.instagram.com/nurdrageyoutube/
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Make Silver Nitrate from Silver and Nitric Acid (Revisited)
In this video we revisit making silver nitrate by the classic reaction of silver and nitric acid.
Related videos:
The original video of making silver nitrate: https://www.youtube.com/watch?v=d6hPgGV_qAg
Very simple silver photography: https://www.youtube.com/watch?v=8e0-AbwBDYM
Silver conductive ink: https://www.youtube.com/watch?v=EBlqPS8boLI
Silver mirrors: https://www.youtube.com/watch?v=hUX_cpFWNso
Donate to NurdRage!
Through Patreon (preferred): https://www.patreon.com/NurdRage
Glassware generously provided by http://www.alchemylabsupply.com/
Use the discount code "nurdrage" for a 5% discount.
Social media links:
Twitter: https://twitter.com/NurdRage
Instagram: https://www.instagram.com/nurdrageyoutube/
59
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Make p-Toluenesulfonic Acid
In this video we make p-Toluenesulfonic acid from sulfuric acid based drain cleaner and paint thinner containing toluene.
Donate to NurdRage!
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Through Bitcoin: 1NurdRAge7PNR4ULrbrpcYvc9RC4LDp9pS
Glassware generously provided by http://www.alchemylabsupply.com/
Use the discount code "nurdrage" for a 5% discount.
Twitter: https://twitter.com/NurdRage
Reddit: https://www.reddit.com/r/NurdRage/
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43
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How to remove the Coke can from the Coke!
In this video we do something really silly and remove a can from the coke it contains.
To do the demonstration: First get any soft drink can and using sandpaper, sand off the label. Then open the can and suspend it by the tab in 5% hydrochloric acid. The exact concentration is not critical. The can must be opened or it will rupture as the aluminum is removed.
Over the course of an hour, the aluminum in the can will be attacked by the acid and dissolve away. This leaves behind the drink and also a very thin plastic liner inside the can. This liner protects the drink from leaching metals out of the can. Carefully lift the can to reveal the liner still holding the drink.
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Smash glow crystals in a blender
We put triboluminescent, or "Smash Glow" crystals in a blender. Triboluminescence is the effect of light being emitted when something is broken, smashed, or otherwise broken. The substance in this video is a particular type of chemical called triphenylphosphinebis(pyridine)thiocyanato copper(I). Enjoy!
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Gallium-induced structural failure of aluminum baseball bat
In this video we demonstrate the structural failure of an aluminum baseball bat induced by gallium metal. You won't believe the final result!
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Peanut butter glows in the dark
Peanut butter glows in the dark when subjected to strong light. It's very faint and hard to see but a violet laser pointer is strong enough to reveal the effect.
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