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Making Ether with Polyphosphoric Acid
Welcome to the second Fan Follow-Up Episode! In this, I test silica-supported polyphosphoric acid’s ability to condense alcohol into ether.
Testing Polyphosphoric Acid:
Polyphosphoric Acid is said to be a powerful dehydrating agent useful in many condensation reactions. I test this literature by implementing this catalyst in my ether synthesis.
Source:
https://www.mdpi.com/1420-3049/18/2/1869
Gear Used In This Video:
â–³ 700W 110V Soldering Station Hot Plate: https://amzn.to/4c3bQ52
â–³ StonyLab 3 Way Distilling Thermometer Adapter: https://amzn.to/3VztlEJ
â–³ Borosilicate Glass Liebig Condenser with 24/40 Joint 500mm: https://amzn.to/3Vo04fM
â–³ Glass Vacuum Take Off Adapter, 105 Degree Bent, Short Stem: https://amzn.to/4c5apmD
â–³ 500mL Single Neck 1 Neck Round Bottom Flask: https://amzn.to/4bX3Gvr
â–³ QWORK Glass 1000ml Single Neck Flat Bottom Boiling Flask: https://amzn.to/3KqCNnq
â–³ Submersible Pump 200GPH Ultra Quiet: https://amzn.to/4aQ4vEB
â–³ Allen Tech PTFE Teflon tub: https://amzn.to/4e7JyYE
â–³ Custom Embroidered Mens Medical Laboratory Coats - Add Your Name or Text: https://amzn.to/3yJOQJN
â–³ Flexzilla Pro GC400PL Heavy Duty Cleaning, Neoprene: https://amzn.to/4bxQXPr
To see more amazing content, check out Molecular Playground down here:
https://www.youtube.com/channel/UCdOU-9RkIlms9Syq5513BXg?sub_confirmation=1
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