Chlorobutanol Synthesis

TheBackyardScientistPublished: June 21, 2016Updated: June 22, 20163 views
Published: June 21, 2016Updated: June 22, 2016

Recrystallize in enough methanol to dissolve, then place in refrigerator for large crystals (4 days) OR freezer for smaller (4-8 hours). do multiple smaller pulls.

90ml acetone
10ml chloroform
1-2gm NaOH
Yield~ 4gm

Please note this is not safe for consumption. It may contain small amounts of un r

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